In this paper a systematic study of individual single-walled and multi-walled carbon nanotubes was performed by Raman spectroscopy and high-resolution electron microscopy. We have presented the geometrical and electronic structure analysis on the examples of two tubes: individual single-walled and double-walled nanotubes. The role of different environmental effects and their influence on the final structure assignment are discussed. Moreover, we have shown that the Raman spectroscopy gives reliable estimations of the nanotube diameters and the conductivity. Given a non-destructible character of Raman spectroscopy, we may conclude that it is one of the most efficient methods for structure analysis of carbon nanotubes.
Keywords: Carbon nanotubes, Raman spectroscopy, electron microscopy
The possibility of channeling X-ray fluorescence inside the hollow microvascular at the energy of the exciting radiation in the vicinity SiL2, 3 - absorption edge has been researched. Theoretically obtained the angular distribution of the field passing through the microchannels. The calculation model of inhomogeneous waveguide layer with the generation of X-ray fluorescence inside the walls of the microchannels shows the possibility of escape of radiation at large angles.
Keywords: channeling of X-ray fluorescence, microchannel plates, focusing of X-ray radiation
The article is devoted to the problem of the identification of the Black Sea – Caspian region as a special segment of the World Space in the postbypolar system. The Great Limitrophe conception developed by V.L. Tsymbursky and S.V. Khatuntsev is used as «the structural frame» for understanding modern peculiarities of this region. The author outlines two aspects of its identification: geopolitical and geocivilozational. He also introduces the key concept «limitroph territory» adapting it to the specific region. The key concept involves two other concepts – «shatterbelt» and «(inter)civilizational split zone». The article contains brand new facts on the Black Sea – Caspian region problem.
Keywords: «big political space», geopolitics, Black Sea – Caspian region, Great Limitrophe conception, limitrophe-territory, «shatterbellt», civilizational layer, «(inter)civilizational split zone».
Oxide bronzes MxEO3 (M–Na,K; E – W,Mo) are the inorganic materials for technics and chemical technology. Its properties, for example stability in wide interval of temperatures, are of great practical interest (electrodes for fuel elements, electronic apparatuses and others). In this article the results of studies of thermostability of sodium and potassium tungsten and molybdenum bronzes in atmosphere and vacuum condition at the temperatures range 20-1110°C were found. The samples are prepared by electrolysis of melts of sodium and potassium isopolytungstates and molybdates. Dates for bronzes Na0.92WO3 , Na0.68WO3 , Na0.53WO3 , Na0.15MoO3, K0.3MoO3 were characterized by the termogravimetric-differential- thermal analysis (TG-DTA). Regions of stability of Na0.92WO3 : 20-700°C , of MxMoO3 : 300-500°C were founded. Conclusion about correlation of nonstoichiometry of chemical composition of EOx bronzes and oxides, which making important role in formation of less - common metal bronzes structure.
Keywords: oxide alkali bronzes, tungsten, molybdenum, thermostability, nonstoichiometry, thermal analysis
In order to improve techniques of minimally invasive total knee arthroplasty (IEAC) based on anatomical studies, we have developed a mathematical model and a computer program IEAC preoperative planning that takes into account the anthropometric data of the patient (body type, size patellar index Insall-Salvati), type and size of prosthesis and allows to calculate minimal incision and maximum elongation wound during surgery. Use of this software improves the accuracy of the planning and preparation of surgery, to improve the accuracy of implantation of the prosthesis.
Keywords: minimally invasive replacement of knee joint, computer modelling, preoperative planning, computer software preoperative planning
This article is related to technological problems of cavities with kamufletnyh explosions, during which the temperature in the cavity greatly exceeds the initial temperature of the array. Often these cavities are created in an array of rock salt. Because the salt even at light loads demonstrate expressive flow properties, it is interesting solution to the problem of creep salt massif with a cavity under the action of a force (pressure inside the cavity and the pressure of the soil), and thermal loads.
Keywords: heterogeneity, creep, highly elastic deformation, hydrochloric array coupling equation, the integral relations
This article related to the technological problem. Books and manuscripts are subjected to natural aging due to the fragility of the raw materials, the deterioration of the conditions of storage, as well as losses of fragments due to repeated or careless operation. Therefore, for libraries, archives and museums is particularly important in matters of preservation of documents not only the process of conservation, but the recovery of the lost fragments.
Keywords: technology, restoration, conservation, listodolivochnye machines, vacuum table, the machine for making pulp
The article describes the three main causes of marriage exactly litena production. Suggests ways to address them.
Keywords: Marriage in precision casting, a type of marriage, the reasons for marriage.
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The construction of a two-dimensional tiling by a specific projection of three-dimensional cubic lattice is considered. Different a periodic tiling’s, consisting of equal rhombi, are obtained by different choice of the projection region. They are ordinary a periodic tiling, having local elements of symmetry group С6v and chiral trigonal stacking, built like chiral pentagonal Penrose’s quasilattice [1], which occurs in virus cap sides.
Keywords: Quasicrystal, quasilattice, two-dimensionalquasicrystal, chiral quasicrystal.
In this paper, we describe fully all the stages of plastic forms. The advantages of using "Pentelast-710." Due to its ease of use, environmental, security, diversity of products offered, two-component silicone rubber is a promising structural material.
Keywords: "Pentelast-710" Viksint U-18, platemaking technology.
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